Content of the repository:
- Pulse_parameters.xlsx
All pulse parameters for assignment and dynamics spectra recorded in this study.
- Scripts_submission.zip
Code to fit overall tumbling from 15N-TRACT experiment, as well as the analysis of anisotropic tumbling. Fits of 3Q relaxation to measure order parameters. Calculations and correlations of sovent accessible surface area. Investigation of potential artefacts by external protons. All as described in supplementary section S2.
- FLYA_runs.zip
All ablation and addition runs in FLYA as described in supplementary section S1, as well as an example FLYA run for the assignment of C-detected spectra with H-detected inputs.
- spectra_Bruker.zip
All raw assignment and dynamics spectra used in this study, including pulse sequences (Bruker format).
- Titration_data.zip
Spectra and peaklists of the oxamate titration.