---
_id: '8484'
abstract:
- lang: eng
  text: A series of sequential, intra-residue, and bi-directional BEST H–N–CA, H–N–CO,
    and H–N–CB pulse sequences is presented that extends the BEST concept introduced
    recently for fast multidimensional protein NMR [Schanda et al., J. Am. Chem. Soc.
    128 (2006) 9042] to the complete set of experiments required for sequential resonance
    assignment. We demonstrate for the protein ubiquitin that 3D BEST H–N–C correlation
    spectra can be recorded on a 600 MHz NMR spectrometer equipped with a cryogenic
    probe in only a few minutes of acquisition time with sufficient sensitivity to
    detect all expected cross peaks.
article_processing_charge: No
article_type: letter_note
author:
- first_name: Ewen
  full_name: Lescop, Ewen
  last_name: Lescop
- first_name: Paul
  full_name: Schanda, Paul
  id: 7B541462-FAF6-11E9-A490-E8DFE5697425
  last_name: Schanda
  orcid: 0000-0002-9350-7606
- first_name: Bernhard
  full_name: Brutscher, Bernhard
  last_name: Brutscher
citation:
  ama: Lescop E, Schanda P, Brutscher B. A set of BEST triple-resonance experiments
    for time-optimized protein resonance assignment. <i>Journal of Magnetic Resonance</i>.
    2007;187(1):163-169. doi:<a href="https://doi.org/10.1016/j.jmr.2007.04.002">10.1016/j.jmr.2007.04.002</a>
  apa: Lescop, E., Schanda, P., &#38; Brutscher, B. (2007). A set of BEST triple-resonance
    experiments for time-optimized protein resonance assignment. <i>Journal of Magnetic
    Resonance</i>. Elsevier. <a href="https://doi.org/10.1016/j.jmr.2007.04.002">https://doi.org/10.1016/j.jmr.2007.04.002</a>
  chicago: Lescop, Ewen, Paul Schanda, and Bernhard Brutscher. “A Set of BEST Triple-Resonance
    Experiments for Time-Optimized Protein Resonance Assignment.” <i>Journal of Magnetic
    Resonance</i>. Elsevier, 2007. <a href="https://doi.org/10.1016/j.jmr.2007.04.002">https://doi.org/10.1016/j.jmr.2007.04.002</a>.
  ieee: E. Lescop, P. Schanda, and B. Brutscher, “A set of BEST triple-resonance experiments
    for time-optimized protein resonance assignment,” <i>Journal of Magnetic Resonance</i>,
    vol. 187, no. 1. Elsevier, pp. 163–169, 2007.
  ista: Lescop E, Schanda P, Brutscher B. 2007. A set of BEST triple-resonance experiments
    for time-optimized protein resonance assignment. Journal of Magnetic Resonance.
    187(1), 163–169.
  mla: Lescop, Ewen, et al. “A Set of BEST Triple-Resonance Experiments for Time-Optimized
    Protein Resonance Assignment.” <i>Journal of Magnetic Resonance</i>, vol. 187,
    no. 1, Elsevier, 2007, pp. 163–69, doi:<a href="https://doi.org/10.1016/j.jmr.2007.04.002">10.1016/j.jmr.2007.04.002</a>.
  short: E. Lescop, P. Schanda, B. Brutscher, Journal of Magnetic Resonance 187 (2007)
    163–169.
date_created: 2020-09-18T10:13:02Z
date_published: 2007-07-01T00:00:00Z
date_updated: 2021-01-12T08:19:35Z
day: '01'
doi: 10.1016/j.jmr.2007.04.002
extern: '1'
intvolume: '       187'
issue: '1'
language:
- iso: eng
month: '07'
oa_version: None
page: 163-169
publication: Journal of Magnetic Resonance
publication_identifier:
  issn:
  - 1090-7807
publication_status: published
publisher: Elsevier
quality_controlled: '1'
status: public
title: A set of BEST triple-resonance experiments for time-optimized protein resonance
  assignment
type: journal_article
user_id: 2DF688A6-F248-11E8-B48F-1D18A9856A87
volume: 187
year: '2007'
...